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Title: Synthesis, X-ray crystal structure and spectroscopic studies of benzothiazole Schiff base
Authors: Demircioğlu, Yasemin Süzen
Sakarya, H.C.
Süzen, Y.
Keywords: Benzothiazole
Ethyl L-lactate
Schiff base
X-ray structure
Issue Date: 2020
Publisher: Bulgarian Academy of Sciences
Abstract: The new Schiff base 3 was synthesized by reacting 6-methyl-2-aminobenzothiazole and 2-methoxy-1-naphtaldehyde in ethyl L- lactate as a green solvent. Compound 3 was characterized by FT-IR, 1H NMR, 13C NMR, single crystal X-ray diffraction study and elemental analysis. The compound crystallizes in the monoclinic space group P21/n, with a= 8.1077(15), b=17.302(3), c=22.790(4) Å, ?= 95.799(7), V= 3180.7(1) Å3, absorption coefficient= 0.212 mm-1. The asymmetric unit contains two crystallographically independent molecules with intramolecular C-H···N and intermolecular C-H···Cg interactions. © 2020 Bulgarian Academy of Sciences, Union of Chemists in Bulgaria
ISSN: 0861-9808
Appears in Collections:Porsuk Meslek Yüksekokulu Yayın Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu

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